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Finally, the residue was dissolved in 50 L mobile phase (acetonitrile/water (80/20) with 0.05% v/v acetic acid) and analysed by LC/MS was carried out on a Agilent Technologies 1290 Infinity II UHPLC module coupled to a 6475 LC/TQ(triple quadrupole) tandem mass spectrometer controlled by Agilent OpenLab Control Panel (6475A) software (Agilent Technologies, Santa Clara, CA, USA)